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Year 2023, Volume: 26, 416 - 419, 30.12.2023

Resat Can Ozden Mustafa Anık

https://doi.org/10.55549/epstem.1411043

Abstract

References

  • Adegoke, K. A., & Maxakato, N. W. (2022). Porous metal oxide electrocatalytic nanomaterials for energy conversion: Oxygen defects and selection techniques. Coordination Chemistry Reviews, 457, 214389.
  • Amirkhanyan, N., Kharatyan, S., Manukyan, K., & Aprahamian, A. (2020). Thermodynamics and kinetics of solution combustion synthesis: Ni(NO3)2 + fuels systems. Combustion and Flame, 221, 110–119.
  • Chen, H., Zhao, Y., Yang, M., He, J., Chu, P. K., Zhang, J., & Wu, S. (2010). Glycine-assisted hydrothermal synthesis of peculiar porous α-Fe2O3 nanospheres with excellent gas-sensing properties. Analytica Chimica Acta, 659(1–2), 266–273.

Glycine-Assisted Synthesis of High Surface Area (FeMnCrCoZn)3O4 Microsheets

Year 2023, Volume: 26, 416 - 419, 30.12.2023

Resat Can Ozden Mustafa Anık

https://doi.org/10.55549/epstem.1411043

Abstract

To meet the current demands for energy storage and conversion, it is crucial to develop newly designed materials. Porous metal oxides with a high specific surface area and controllable porosity are promising electrode materials for electrochemical energy storage and conversion applications. Furthermore, porous materials offer a unique combination of structural, chemical and physical properties. In this study, porous high-entropy oxides (FeMnCrCoZn)₃O₄ were synthesized through soft chemistry route, employing glycine as a pore-forming agent, followed by calcination at various temperatures (500 °C, 600 °C and 700 °C) for 4h. The obtained samples were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM) techniques. It was observed that the samples were successfully synthesized in porous microsheet morphology and as a single phase in the spinel crystal structure. Additionally, the effect of different calcination temperatures on the pore structure has been investigated.

Keywords

High-entropy oxides Porous metal oxides Template-free method

References

  • Adegoke, K. A., & Maxakato, N. W. (2022). Porous metal oxide electrocatalytic nanomaterials for energy conversion: Oxygen defects and selection techniques. Coordination Chemistry Reviews, 457, 214389.
  • Amirkhanyan, N., Kharatyan, S., Manukyan, K., & Aprahamian, A. (2020). Thermodynamics and kinetics of solution combustion synthesis: Ni(NO3)2 + fuels systems. Combustion and Flame, 221, 110–119.
  • Chen, H., Zhao, Y., Yang, M., He, J., Chu, P. K., Zhang, J., & Wu, S. (2010). Glycine-assisted hydrothermal synthesis of peculiar porous α-Fe2O3 nanospheres with excellent gas-sensing properties. Analytica Chimica Acta, 659(1–2), 266–273.
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Details

Primary Language English
Subjects Environmental and Sustainable Processes
Journal Section Articles
Authors

Resat Can Ozden

Mustafa Anık

Early Pub Date December 27, 2023
Publication Date December 30, 2023
Published in Issue Year 2023 Volume: 26

Cite

APA Ozden, R. C., & Anık, M. (2023). Glycine-Assisted Synthesis of High Surface Area (FeMnCrCoZn)3O4 Microsheets. The Eurasia Proceedings of Science Technology Engineering and Mathematics, 26, 416-419. https://doi.org/10.55549/epstem.1411043
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